← Back to search

1b59

COMPLEX OF HUMAN METHIONINE AMINOPEPTIDASE-2 COMPLEXED WITH OVALICIN

Method: X-RAY DIFFRACTION D_max: 66.6 Å Quality: GOOD

SAXS Profile

P(r) Distribution

▼

1. Structure Basics

entry_id	1b59
deposition_date	1999-01-13
title	COMPLEX OF HUMAN METHIONINE AMINOPEPTIDASE-2 COMPLEXED WITH OVALICIN
keywords	ANGIOGENESIS INHIBITOR, HYDROLASE; HYDROLASE
method	X-RAY DIFFRACTION

▼

Download Data

SAXS curve (.dat) P(r) distribution (.pr.out) Structure (CIF)

▼

2. SAXS Parameters (CRYSOL)

rg_guinier	21.01 Å
rg_electron	20.04 Å
i0	28343700.00
molecular_weight	40180.0 kDa
excluded_volume	50005 Å³
envelope_volume	57166 Å³
shell_volume	23213 Å³
envelope_diameter	68.7 Å
shell_rg	27.36 Å
envelope_rg	20.64 Å
shape_rg	20.04 Å
total_rg	20.99 Å
total_atoms	2809
n_residues	355
n_harmonics	20
q_range	— – 0.5000 Å⁻¹
n_points	101
shell_type	directional
solvent_density	0.3340 e/Å³
contrast_shell	0.0300 e/Å³
crysol_version	4.1.3

▼

3. P(r) Analysis (GNOM)

dmax	66.6 Å
rg_real	20.89 Å
rg_real_error	0.30 Å
i0_real	2.8340e+07
i0_real_error	2.9850e+05
rg_reciprocal	20.91 Å
i0_reciprocal	28340000.0000
total_estimate	0.8973
solution_quality	GOOD a GOOD solution
n_peaks	2
r_peak_primary	26.1 Å
skewness	0.175
kurtosis	-0.449
angular_range	— – 0.3800 Å⁻¹
current_alpha	0.0000
highest_alpha	10110000.0000
n_real_points	70
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.891; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.994; Smooth: 0.993

▶

4. Crystallography & Experiment

▶

5. Entities & Polymer Info (4)

Entity 1 polymer

description	PROTEIN (METHIONINE AMINOPEPTIDASE)
formula_weight	41453.1 kDa
ec_number	3.4.11.18
src_method	man
entity_count	1

Polymer

type	polypeptide(L)
strand_id	A
atom_count	3022

PKVQTDPPSVPICDLYPNGVFPKGQECEYPPTQDGRTAAWRTTSEEKKALDQASEEIWNDFREAAEAHRQVRKYVMSWIKPGMTMIEICEKLEDCSRKLIKENGLNAGLAFPTGCSLNNCAAHYTPNAGDTTVLQYDDICKIDFGTHISGRIIDCAFTVTFNPKYDTLLKAVKDATNTGIKCAGIDVRLCDVGEAIQEVMESYEVEIDGKTYQVKPIRNLNGHSIGQYRIHAGKTVPIVKGGEATRMEEGEVYAIETFGSTGKGVVHDDMECSHYMKNFDVGHVPIRLPRTKHLLNVINENFGTLAFCRRWLDRLGESKYLMALKNLCDLGIVDPYPPLCDIKGSYTAQFEHTILLRPTCKEVVSRGDDY

Source

organism	Homo sapiens
common_name	human
ncbi_taxonomy_id	9606
host_organism	Spodoptera frugiperda MNPV

Entity 2 non-polymer

description	COBALT (II) ION
formula_weight	58.9 kDa
src_method	syn
entity_count	2

Entity 3 non-polymer

description	3,4-DIHYDROXY-2-METHOXY-4-METHYL-3-[2-METHYL-3-(3-METHYL-BUT-2-ENYL) -OXIRANYL]-CYCLOHEXANONE
formula_weight	298.4 kDa
src_method	syn
entity_count	1

Entity 4 water

description	water
formula_weight	18.0 kDa
src_method	nat
entity_count	213

▶

6. Citations (1)

▶

length_a	89.723 Å
length_b	99.108 Å
length_c	101.292 Å
angle_alpha	90.00 °
angle_beta	90.00 °
angle_gamma	90.00 °
z_pdb	8

space_group	C 2 2 21
int_tables_number	20
crystal_system	—

resolution	1.800 Å
resolution_low	6.000 Å
r_factor	0.1780
r_work	0.1780
r_free	0.2220

fit	/app/data/saxs_computation/b5/1b59/1b59.fit
pddf	/app/data/pr_computation/b5/1b59/1b59.pr.out
profile	/app/data/saxs_computation/b5/1b59/1b59.dat

COMPLEX OF HUMAN METHIONINE AMINOPEPTIDASE-2 COMPLEXED WITH OVALICIN

SAXS Profile

P(r) Distribution

1. Structure Basics

Download Data

2. SAXS Parameters (CRYSOL)

3. P(r) Analysis (GNOM)

4. Crystallography & Experiment

Unit Cell

Symmetry

Refinement

Diffraction