1fdl

CRYSTALLOGRAPHIC REFINEMENT OF THE THREE-DIMENSIONAL STRUCTURE OF THE FAB D1.3-LYSOZYME COMPLEX AT 2.5-ANGSTROMS RESOLUTION

Method: X-RAY DIFFRACTION Dmax: 111.0 Å Quality: GOOD

SAXS 散射曲线 SAXS Profile

SAXS profile for 1fdl

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1fdl
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1fdl
沉积日期 deposition_date1990-08-27
结构标题 titleCRYSTALLOGRAPHIC REFINEMENT OF THE THREE-DIMENSIONAL STRUCTURE OF THE FAB D1.3-LYSOZYME COMPLEX AT 2.5-ANGSTROMS RESOLUTION
关键词 keywordsCOMPLEX (ANTIBODY-ANTIGEN); COMPLEX (ANTIBODY-ANTIGEN)
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier31.25
回转半径 Rg (电子) rg_electron30.85
零角强度 I(0) i065258600.00
分子量 molecular_weight61356.0 kDa
排除体积 excluded_volume75721 ų
包络体积 envelope_volume97646 ų
水化壳体积 shell_volume28927 ų
包络直径 envelope_diameter111.8
壳层 Rg shell_rg34.89
包络 Rg envelope_rg30.67
形状 Rg shape_rg30.79
总 Rg total_rg31.36
总原子数 total_atoms4309
残基数 n_residues561
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax111.0
Rg (实空间) rg_real31.64
Rg 误差 (实空间) rg_real_error1.19
I(0) (实空间) i0_real6.5260e+07
I(0) 误差 (实空间) i0_real_error1.1530e+06
Rg (倒空间) rg_reciprocal31.48
I(0) (倒空间) i0_reciprocal65250000.0000
解质量估计 total_estimate0.8056
解质量评级 solution_quality GOOD a GOOD solution
P(r) 峰数 n_peaks0
主峰位置 r_peak_primary
偏度 Skewness skewness0.609
峰度 Kurtosis kurtosis-0.167
角度范围 angular_range— – 0.2550 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha10520000.0000
实空间数据点数 n_real_points52
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.695; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.555; Smooth: 0.830

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (3)

6. 折叠分类 (SCOP + CATH) 10 domains

SCOP 2.08 (5 domains)

结构域编号 domain_idd1fdlh1
类 Class classb — All beta proteins
折叠类型 Fold foldb.1 — Immunoglobulin-like beta-sandwich
超家族 Superfamily superfamilyb.1.1 — Immunoglobulin
家族 Family familyb.1.1.1 — V set domains (antibody variable domain-like)
结构域编号 domain_idd1fdlh2
类 Class classb — All beta proteins
折叠类型 Fold foldb.1 — Immunoglobulin-like beta-sandwich
超家族 Superfamily superfamilyb.1.1 — Immunoglobulin
家族 Family familyb.1.1.2 — C1 set domains (antibody constant domain-like)
结构域编号 domain_idd1fdll1
类 Class classb — All beta proteins
折叠类型 Fold foldb.1 — Immunoglobulin-like beta-sandwich
超家族 Superfamily superfamilyb.1.1 — Immunoglobulin
家族 Family familyb.1.1.1 — V set domains (antibody variable domain-like)
结构域编号 domain_idd1fdll2
类 Class classb — All beta proteins
折叠类型 Fold foldb.1 — Immunoglobulin-like beta-sandwich
超家族 Superfamily superfamilyb.1.1 — Immunoglobulin
家族 Family familyb.1.1.2 — C1 set domains (antibody constant domain-like)
结构域编号 domain_idd1fdly_
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.2 — Lysozyme-like
超家族 Superfamily superfamilyd.2.1 — Lysozyme-like
家族 Family familyd.2.1.2 — C-type lysozyme

CATH v4.4 (5 domains)

结构域编号 domain_id1fdlH01
类 Class class2 — Mainly Beta
架构 Architecture architecture60 — Sandwich
拓扑 Topology topology40 — Immunoglobulin-like
同源超家族 H-superfamily homologous superfamily10 — Immunoglobulins
结构域编号 domain_id1fdlH02
类 Class class2 — Mainly Beta
架构 Architecture architecture60 — Sandwich
拓扑 Topology topology40 — Immunoglobulin-like
同源超家族 H-superfamily homologous superfamily10 — Immunoglobulins
结构域编号 domain_id1fdlL01
类 Class class2 — Mainly Beta
架构 Architecture architecture60 — Sandwich
拓扑 Topology topology40 — Immunoglobulin-like
同源超家族 H-superfamily homologous superfamily10 — Immunoglobulins
结构域编号 domain_id1fdlL02
类 Class class2 — Mainly Beta
架构 Architecture architecture60 — Sandwich
拓扑 Topology topology40 — Immunoglobulin-like
同源超家族 H-superfamily homologous superfamily10 — Immunoglobulins
结构域编号 domain_id1fdlY00
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology530 — Lysozyme
同源超家族 H-superfamily homologous superfamily10

7. 引用文献 (1)

8. 文件与曲线 (10)