RAT TYPE II ADENYLYL CYCLASE C2 DOMAIN/FORSKOLIN COMPLEX

Method: X-RAY DIFFRACTION D_max: 68.9 Å Quality: EXCELLENT

SAXS Profile

P(r) Distribution

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1. Structure Basics

entry_id	1ab8
deposition_date	1997-02-04
title	RAT TYPE II ADENYLYL CYCLASE C2 DOMAIN/FORSKOLIN COMPLEX
keywords	LYASE, ADENYLYL CYCLASE, PLASMID, COMPLEX (TRANSFERASE-INHIBITOR); LYASE
method	X-RAY DIFFRACTION

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Download Data

SAXS curve (.dat) P(r) distribution (.pr.out) Structure (CIF)

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2. SAXS Parameters (CRYSOL)

rg_guinier	21.87 Å
rg_electron	20.73 Å
i0	24673900.00
molecular_weight	39435.0 kDa
excluded_volume	49862 Å³
envelope_volume	56720 Å³
shell_volume	22537 Å³
envelope_diameter	68.9 Å
shell_rg	27.52 Å
envelope_rg	20.93 Å
shape_rg	20.73 Å
total_rg	21.59 Å
total_atoms	2772
n_residues	353
n_harmonics	20
q_range	— – 0.5000 Å⁻¹
n_points	101
shell_type	directional
solvent_density	0.3340 e/Å³
contrast_shell	0.0300 e/Å³
crysol_version	4.1.3

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3. P(r) Analysis (GNOM)

dmax	68.9 Å
rg_real	21.75 Å
rg_real_error	0.51 Å
i0_real	2.4670e+07
i0_real_error	3.2560e+05
rg_reciprocal	21.77 Å
i0_reciprocal	24670000.0000
total_estimate	0.9045
solution_quality	EXCELLENT a EXCELLENT solution
n_peaks	2
r_peak_primary	25.7 Å
skewness	0.168
kurtosis	-0.506
angular_range	— – 0.3650 Å⁻¹
current_alpha	0.0000
highest_alpha	5932000.0000
n_real_points	68
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.922; Stabil: 0.999; Sysdev: 1.000; Positv: 1.000; Valcen: 1.000; Smooth: 0.990

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4. Crystallography & Experiment

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5. Entities & Polymer Info (3)

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6. Citations (1)

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length_a	81.300 Å
length_b	81.300 Å
length_c	180.500 Å
angle_alpha	90.00 °
angle_beta	90.00 °
angle_gamma	90.00 °
z_pdb	16

space_group	P 43 21 2
int_tables_number	96
crystal_system	—

resolution	2.200 Å
resolution_low	6.000 Å
r_factor	0.2190
r_work	0.2190
r_free	0.2840

description	ADENYLYL CYCLASE
formula_weight	24447.8 kDa
ec_number	4.6.1.1
src_method	man
entity_count	2

type	polypeptide(L)
strand_id	A,B
atom_count	2885

RAT TYPE II ADENYLYL CYCLASE C2 DOMAIN/FORSKOLIN COMPLEX

SAXS Profile

P(r) Distribution

1. Structure Basics

Download Data

2. SAXS Parameters (CRYSOL)

3. P(r) Analysis (GNOM)

4. Crystallography & Experiment

Unit Cell

Symmetry

Refinement

Diffraction

5. Entities & Polymer Info (3)

Entity 1 polymer

Polymer

Source

Entity 2 non-polymer

Entity 3 water

6. Citations (1)

7. Files & Curves (10)

Files (7)

Curves (3)

organism	Rattus norvegicus
common_name	Norway rat
ncbi_taxonomy_id	10116
host_organism	Escherichia coli BL21(DE3)

description	FORSKOLIN
formula_weight	410.5 kDa
src_method	syn
entity_count	2

description	water
formula_weight	18.0 kDa
src_method	nat
entity_count	113

fit	/app/data/saxs_computation/ab/1ab8/1ab8.fit
pddf	/app/data/pr_computation/ab/1ab8/1ab8.pr.out
profile	/app/data/saxs_computation/ab/1ab8/1ab8.dat