X-RAY STRUCTURE OF THE C-TERMINAL ULP1 PROTEASE DOMAIN IN COMPLEX WITH SMT3, THE YEAST ORTHOLOG OF SUMO.

entry_id	1euv
deposition_date	2000-04-17
title	X-RAY STRUCTURE OF THE C-TERMINAL ULP1 PROTEASE DOMAIN IN COMPLEX WITH SMT3, THE YEAST ORTHOLOG OF SUMO.
keywords	;SUMO HYDROLASE, UBIQUITIN-LIKE PROTEASE 1, SMT3 HYDROLASE DESUMOYLATING ENZYME, CYSTEINE PROTEASE, SUMO PROCESSING ENZYME, SMT3 PROCESSING ENZYME, NABH4, THIOHEMIACETAL, COVALENT PROTEASE ADDUCT, HYDROLASE ;; HYDROLASE
method	X-RAY DIFFRACTION

rg_guinier	20.47 Å
rg_electron	19.31 Å
i0	20777600.00
molecular_weight	34366.0 kDa
excluded_volume	42969 ų
envelope_volume	49634 ų
shell_volume	21206 ų
envelope_diameter	66.8 Å
shell_rg	26.04 Å
envelope_rg	19.66 Å
shape_rg	19.30 Å
total_rg	20.28 Å
total_atoms	2417
n_residues	300
n_harmonics	20
q_range	— – 0.5000 Å−1
n_points	101
shell_type	directional
solvent_density	0.3340 e/ų
contrast_shell	0.0300 e/ų
crysol_version	4.1.3

dmax	65.8 Å
rg_real	20.37 Å
rg_real_error	0.43 Å
i0_real	2.0780e+07
i0_real_error	2.7520e+05
rg_reciprocal	20.38 Å
i0_reciprocal	20780000.0000
total_estimate	0.8153
solution_quality	GOOD a GOOD solution
n_peaks	2
r_peak_primary	24.4 Å
skewness	0.203
kurtosis	-0.417
angular_range	— – 0.3900 Å−1
current_alpha	0.0000
highest_alpha	5063000.0000
n_real_points	71
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.867; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.995; Smooth: 0.000

Unit Cell

length_a	125.774 Å
length_b	53.167 Å
length_c	54.262 Å
angle_alpha	90.00 °
angle_beta	90.00 °
angle_gamma	90.00 °
z_pdb	4

Symmetry

space_group	P 21 21 2
int_tables_number	18
crystal_system	—

Refinement

resolution	1.600 Å
resolution_low	25.000 Å
r_factor	0.1930
r_work	0.1900
r_free	0.2510

Diffraction

temperature

100.0 K

Files (7)

• pr_distribution /app/data/pr_computation/eu/1euv/pr_distribution.json
• pr_output /app/data/pr_computation/eu/1euv/1euv.pr.out
• pr_plot /app/data/visualization/pr_computation/eu/1euv/1euv_pr_distribution.png
• saxs_curve_dat /app/data/saxs_computation/eu/1euv/1euv.dat
• saxs_fit /app/data/saxs_computation/eu/1euv/1euv.fit
• saxs_log /app/data/saxs_computation/eu/1euv/1euv.log
• saxs_plot /app/data/visualization/saxs_computation/eu/1euv/1euv_saxs_profile.png

Curves (3)

fit	/app/data/saxs_computation/eu/1euv/1euv.fit
pddf	/app/data/pr_computation/eu/1euv/1euv.pr.out
profile	/app/data/saxs_computation/eu/1euv/1euv.dat